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This study demonstrated the technical potential for the large-scale co-production of sugars, lignosulfonates, cellulose, and cellulose nanocrystals. Ball-milled woods with two particle sizes were prepared by ball milling for 80min or 120min (BMW80, BMW120) and then enzymatically hydrolyzed. 78.3% cellulose conversion of BMW120 was achieved, which was three times as high as the conversion of BMW80.
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Grinding test were performed in an XMQ-Φ240 × 90 laboratory-scale conical ball mill (Wuan Exploring Machinery Factory, Wuhan, China). For the wet- and dry-grinding tests, the ball diameter, fractional ball filling, and fractional powder filling were 35 mm, 19.31%, and 6.80%.
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Determination and scale up of the milling parameters of a . An experimental laboratory scale ball mill available at the University of Lubumbashi was used in this research work The ball mill measured 0.305 m in diameter and 0.127 in length It was driven by an asynchronous motor rated with power close to 10 kW A schematic of the experimental laboratory ball mill used is shown in Fig 3.
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In the same manner, the energy consumption of product with d 80 = 81 μm by using the laboratory scale ball mill was 72.73 kWh/t after 24 min of grinding. It can be clearly seen that the d 80 size of the fossil fuel reduced from 2100 μm to 1130 μm after a 4 min grinding period in the ball mill grinding tests.
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Ball/Rod mill Literature The Ball/Rod mills are meant for producing fine particle size reduction through attrition and compressive forces at the grain size level. They are the most effective laboratory mills for batch-wise, rapid grinding of medium-hard to very hard samples down to finest particle sizes.
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The developed ball-milling method enabled large-scale synthesis, that over 4.7 g of Co-SNC can be produced in one pot. In benzylamine coupling reaction, Co-SNC exhibited the highest conversion of 97.5 % with 99 % selectivity toward N-benzylidenebenzylamine in 10 h among various Co catalysts.
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